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Journal Articles

Analysis and mapping of detailed inner information of crystalline grain by wavelength-resolved neutron transmission imaging with individual Bragg-dip profile-fitting analysis

Sakurai, Yosuke*; Sato, Hirotaka*; Adachi, Nozomu*; Morooka, Satoshi; Todaka, Yoshikazu*; Kamiyama, Takashi*

Applied Sciences (Internet), 11(11), p.5219_1 - 5219_17, 2021/06

 Times Cited Count:3 Percentile:41.12(Chemistry, Multidisciplinary)

Journal Articles

Effects of grain size on ultrasonic attenuation in type 316L stainless steel

Wan, T.; Naoe, Takashi; Wakui, Takashi; Futakawa, Masatoshi; Obayashi, Hironari; Sasa, Toshinobu

Materials, 10(7), p.753_1 - 753_17, 2017/07

AA2017-0189.pdf:2.65MB

 Times Cited Count:23 Percentile:72.44(Chemistry, Physical)

Journal Articles

Effects of ultrastrong gravitational field on the crystalline state of a Bi-Sb alloy

Huang, X.*; Mashimo, Tsutomu; Ono, Masao; Tomita, Takeshi; Sawai, Tomotsugu; Osakabe, Toyotaka; Mori, Nobuo*

Journal of Applied Physics, 96(3), p.1336 - 1340, 2004/08

 Times Cited Count:11 Percentile:42.73(Physics, Applied)

Mega-gravity field experiments were performed on the Bi$$_{70}$$Sb$$_{30}$$(atomic percent) alloy and pure Bi below their melting points, to investigate the change in crystalline state. For the alloy centrifuged at 191-205 $$^{circ}$$C, no change in composition was observed, and the grain sizes of the crystals decreased from several mm to tens of $$mu$$m, while no distinct change in grain size was observed for the centrifuged pure Bi. The alloy centrifuged at 220-240 $$^{circ}$$C consisted of two regions with different morphologies-fine-grained crystals with grain sizes around tens of $$mu$$m in the low gravity region, and large crystals with grain sizes several mm long and hundreds of $$mu$$m wide along the direction of gravity in the high gravity region, where sedimentation of atoms was confirmed. The large crystals with hexagonal structures were formed by preferential crystal growth roughly along the c axes, and a large strain that increased as the gravitational field increased existed inside these crystals. Formation of this anomalous crystal state might be correlated with the sedimentation of atoms.

Journal Articles

Energetics of segregation and embrittling potency for non-transition elements in the Ni $$Sigma$$5 (012) symmetrical tilt grain boundary; A First-principles study

Yamaguchi, Masatake; Shiga, Motoyuki; Kaburaki, Hideo

Journal of Physics; Condensed Matter, 16(23), p.3933 - 3956, 2004/06

 Times Cited Count:89 Percentile:92.91(Physics, Condensed Matter)

A series of non-transition elements bound to the Ni $$Sigma$$5(012) symmetrical tilt grain boundary (GB) and the (012) free surface (FS) systems has been studied by first-principles calculation using WIEN2k code. The multilayer relaxations in presence/absence of the solutes are determined by the force minimization. The binding energies at some GB/FS/bulk sites including both interstitial and substitutional sites are calculated for all the non-transition elements between $$_1$$H and $$_{86}$$Rn. The GB/FS segregation energy is obtained by calculating the binding energy difference between the GB/FS site and the bulk site. The embrittling potency energy is obtained by calculating the difference between the GB and FS segregation energies based on Rice-Wang model. Our results show that most of the non-transition elements have negative GB/FS segregation energies. Here, this means that there exists a segregation site in the GB/FS. The embrittling potency energies are positive for most of the solutes. However, some exceptions like Be, B, C, and Si having negative and large embrittling potency can enhance the GB cohesion. Our results are found to be consistent with the experimental findings.

Journal Articles

Damage evaluation techniques for FBR and LWR structural materials based on magnetic and corrosion properties along grain boundaries

Hoshiya, Taiji*; Takaya, Shigeru*; Ueno, Fumiyoshi; Nemoto, Yoshiyuki; Nagae, Yuji*; Miwa, Yukio; Abe, Yasuhiro*; Omi, Masao; Tsukada, Takashi; Aoto, Kazumi*

Transactions of the Materials Research Society of Japan, 29(4), p.1687 - 1690, 2004/06

JAERI and JNC have begun the cooperative research of evaluation techniques of structural material degradation in FBR and LWR, which based on magnetic and corrosion properties along grain boundaries. Magnetic method has been proposed as the one of the non-destructive detection techniques on the early stage of creep-damage before crack initiation for aged structural materials of FBRs. The effects of applied stress on natural magnetization were investigated on paramagnetic stainless steels having creep-damages. On the other hand, corrosion properties and magneto-optical characteristics of ion-irradiated stainless steels in the vicinity of grain boundaries were estimated by AFM and Kerr effect microscope, respectively. These degradations were induced by changes in characteristics in the vicinity of grain boundaries. It is found that the initial level of progressing process of damage can detect changes in magnetic and corrosion properties along grain boundaries of aged and degraded nuclear plants structural materials.

Journal Articles

First-principles study on segregation energy and embrittling potency of hydrogen in Ni$$Sigma$$5(012) tilt grain boundary

Yamaguchi, Masatake; Shiga, Motoyuki; Kaburaki, Hideo

Journal of the Physical Society of Japan, 73(2), p.441 - 449, 2004/02

 Times Cited Count:23 Percentile:71.32(Physics, Multidisciplinary)

The electronic structures of $$Sigma$$5(012) symmetrical tilt grain boundary (GB) and (012) free surface (FS) systems for nickel including hydrogen are calculated by the full-potential linearized augmented plane wave method with the generalized gradient approximation. The difference of the binding energies between the $$Sigma$$5(012)GB/FS site and the inner bulk site is obtained as the GB/FS segregation energy, and the difference between GB and FS segregation energies as the embrittling potency energy. The segregation position of hydrogen atom is determined by the force minimization. We find that hydrogen atom prefers $$Sigma$$5(012)GB to inner bulk energetically by about 0.3 eV/H, while it prefers (012)FS to the GB by about 0.3-0.4 eV/H. The open space at GB may be occupied by an additional interstitial Ni atom since it increases the GB energy by only about 10%. In this case, the GB segregation energy of hydrogen reduces, which makes the segregation difficult. The calculated zero-point energies of hydrogen at inner bulk, GB, and FS sites are within 0.12-0.16eV/H.

Journal Articles

Tensile and impact properties of F82H steel applied to HIP-bond fusion blanket structures

Furuya, Kazuyuki; Wakai, Eiichi; Ando, Masami; Sawai, Tomotsugu; Iwabuchi, Akira*; Nakamura, Kazuyuki; Takeuchi, Hiroshi

Fusion Engineering and Design, 69(1-4), p.385 - 389, 2003/09

 Times Cited Count:23 Percentile:80.61(Nuclear Science & Technology)

In a fusion reactor, a blanket made of a low activation material like F82H is fabricated by solid Hot Isostatic pressing (HIP) joining method. In a previous study, blanket, grain coarsenings were found in a mock-up around HIP-joined region. To verify an effect of the coarsenings on a strength of the HIP-joined region, tensile test and hardness measurement were done. As the results, the tensile strength increased by about 50 MPa, and the elongation decreased by about 4 % in comparison with that of a standard alloy. Though the hardness was almost constant both in the coarsening and a non-coarsening regions, both of these hardness increased by about 5 %. Therefore, it could be judged that change of the tensile property is due to increase of the hardness. On the other hand, tensile and impact tests of a base metal without coarsening resulted in DBTT increase by about 40 K, although the tensile property was nearly equal to that of the joined-region with coarsening. It can be understood that this is the effect of the heat treatments in the fabrication process of the mock-up.

Journal Articles

AFM evaluation of grain boundary corrosion behavior on ion irradiated stainless steel

Nemoto, Yoshiyuki; Miwa, Yukio; Tsukada, Takashi; Tsuji, Hirokazu

JAERI-Conf 2003-001, p.397 - 404, 2003/03

It is essential to evaluate corrosion behavior at grain boundary of irradiated materials for mechanistic understanding of Irradiation assisted stress corrosion cracking (IASCC). However there is no suitable technique to evaluate grain boundary corrosion behavior of irradiated materials. The aim of this work is to develop the measurement method for the grain boundary corrosion behavior of irradiated materials using atomic force microscope (AFM). Ni ion was irradiated to solution annealed Fe-18Cr-12Ni alloy at about 573K. The peak damage level was estimated as 1 dpa. To study relationship of grain boundary character and corrosion behavior, orientation imaging microscope (OIM) observation was conducted. After potentiostatic corrosion procedure, the surface of the specimens were examined with AFM and OIM. Some of grain boundaries were corroded, and these were random coincidence grain boundaries. The depth of the corroded region at grain boundaries was successfully evaluated with AFM in nanometer scale.

Journal Articles

Evaluation of corrosion behavior of ion irradiated stainless steel using atomic force microscope

Nemoto, Yoshiyuki; Miwa, Yukio; Tsuji, Hirokazu; Tsukada, Takashi

Dai-12-Kai MAGDA Konfarensu (Oita) Koen Rombunshu, p.191 - 196, 2003/00

Development and research about analytical method for the study of corrosion behavior of austenitic stainless steel after irradiation was conducted from the point of view for basic study of IASCC (Irradiation Assisted Stress Corrosion Cracking). Ion irradiations were conducted with several irradiation conditions these were irradiation temperature, radiation damage, the contents of helium (He) implantation. AFM (Atomic Force Microscope) was used to evaluate surface condition of irradiated specimens after corrosion procedure. Corrosion condition was developed to obtain good surface condition of irradiated specimens to evaluate corrosion behavior by AFM. It was succeeded and corrosion behavior at inside of grains and grain boundaries of irradiated specimens was obtained. EBSP (Electron Backscatter Diffraction Pattern) was used to evaluate relation of corrosion behavior with grain boundary character. Moreover, relations of corrosion behavior with irradiation condition were discussed.

Journal Articles

Applicability of advanced design method of graphite components by microstructure-based brittle fracture model

Ishihara, Masahiro; Takahashi, Tsuneo*; Hanawa, Satoshi

Transactions of 16th International Conference on Structural Mechanics in Reactor Technology (SMiRT-16) (CD-ROM), 8 Pages, 2001/08

no abstracts in English

Journal Articles

Understanding of mechanical properties of graphite on the basis of mesoscopic microstructure (Review)

Ishihara, Masahiro; Shibata, Taiju; Takahashi, Tsuneo*; Baba, Shinichi; Hoshiya, Taiji

Proceedings of OECD/NEA 2nd Information Exchange Meeting on Basic Studies in the Field of High-temperature Engineering, p.225 - 241, 2001/00

no abstracts in English

JAEA Reports

High temperature corrosion of iron-base and nickel-base alloys for hydrogen production apparatus by thermochemical method in H$$_{2}$$O+SO$$_{3}$$ atmosphere

Kurata, Yuji; Suzuki, Tomio; Shimizu, Saburo

JAERI-Research 2000-011, p.56 - 0, 2000/03

JAERI-Research-2000-011.pdf:14.24MB

no abstracts in English

Journal Articles

Effects of grain size and PCI restraint on the rim structure formation of UO$$_{2}$$ fuels

Une, Katsumi*; Nogita, Kazuhiro*; Suzaka, Yojiro*; Hayashi, Kimio; Ito, Kunio*; Eto, Yoshinori*

International Topical Meeting on Light Water Reactor Fuel Performance, 2, p.775 - 785, 2000/00

no abstracts in English

Journal Articles

Density, porosity and grain size, 2; Irradiated ROX fuels to burn-up of 28%FIMA

Yanagisawa, Kazuaki; Yamashita, Toshiyuki; Kanazawa, Hiroyuki; Amano, Hidetoshi; Muromura, Tadasumi

Journal of Nuclear Science and Technology, 36(12), p.1153 - 1159, 1999/12

 Times Cited Count:0 Percentile:0.01(Nuclear Science & Technology)

no abstracts in English

Journal Articles

Density, porosity and grain size, 1; Unirradiated ROX fules

Yanagisawa, Kazuaki; Yamashita, Toshiyuki; Kanazawa, Hiroyuki; Amano, Hidetoshi; Muromura, Tadasumi

Journal of Nuclear Science and Technology, 36(11), p.1052 - 1063, 1999/11

 Times Cited Count:1 Percentile:13.15(Nuclear Science & Technology)

no abstracts in English

JAEA Reports

A Study on density, porosity and grain size of unirradiated ROX fules and simulated ROX fuels

Yanagisawa, Kazuaki; Omichi, Toshihiko*; Shirasu, Noriko; Yamashita, Toshiyuki; ; Onozawa, Atsushi; ; Kanazawa, Hiroyuki; Kanaitsuka, Fumio; Amano, Hidetoshi

JAERI-Tech 99-044, 46 Pages, 1999/05

JAERI-Tech-99-044.pdf:4.66MB

no abstracts in English

Journal Articles

Effect of stress and impurities on preferential amorphization on grain boundaries in polycrystalline silicon

Takeda, Mitsuhiro*; Onuki, Somei*; Watanabe, Seiichi*; Abe, Hiroaki; Naramoto, Hiroshi; P.R.Okamoto*; N.Q.Lam*

Mat. Res. Soc. Symp. Proc., 540, p.37 - 42, 1999/00

no abstracts in English

Journal Articles

Creep rupture properties of a Ni-Cr-W superalloy in air environment

; Tsuji, Hirokazu; Shindo, Masami; Nakajima, Hajime

Journal of Nuclear Materials, 246(2-3), p.196 - 205, 1997/00

 Times Cited Count:18 Percentile:77.46(Materials Science, Multidisciplinary)

no abstracts in English

JAEA Reports

Creep rupture properties of Ni-Cr-W superalloy in air environment

Kurata, Yuji; Tsuji, Hirokazu; Shindo, Masami; Nakajima, Hajime

JAERI-Research 96-052, 48 Pages, 1996/10

JAERI-Research-96-052.pdf:2.71MB

no abstracts in English

Journal Articles

NDT-observation of superalloy single crystals grown into the gas-turbine blade

Tomimitsu, Hiroshi; *; Aizawa, Kazuya; Yoshinari, Akira*

Journal of the Physical Society of Japan, 65(SUPPL.A), p.252 - 254, 1996/00

no abstracts in English

53 (Records 1-20 displayed on this page)